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Flash and Fire point Test of Bitumen(डामर) (Experimental Procedure, Observations and Result)

 Flash and Fire point test is a safety test conducted on a bituminous material so that it gives an indication of the critical temperature at and above where precautions should be taken to eliminate fire hazards during its applications. Bituminous materials leave out volatiles at high temperature depending upon their grade. These volatile vapors catch fire causing a flash. This condition is very hazardous and it is therefore essential to qualify this temperature for each bitumen grade, so that the paving engineers may restrict the mixing or application temperature well within the limits. Flash and Fire point test is conducted as per IS: 1209.
As per IS: 1209 the definitions of flash and fire point are:

Flash Point: "The flash point of a material is the lowest temperature at which the vapour of substance momentarily takes fire in the form of a flash under specified conditions of test".

Fire Point: "The fire point is the lowest temperature at which the material gets ignited and burns under specified condition of test".

Aim: To determine the flash and fire point of a given bituminous material.


Apparatus: Pensky-Martens closed cup tester, thermometer, heating source, flame exposure.
Procedure:
1.      All parts of the cup are cleaned and dried thoroughly before the test is started.
2.    The material is filled in the cup upto a mark. The lid is placed to close the cup in a closed system. All accessories including thermometer of the specified range are suitably fixed.
3.      The bitumen sample is then heated. The test flame is lit and adjusted in such a way that the size of a bed is of 4mm diameter. The heating of sample is done at a rate of 5° to 6°C per minute. During heating the sample the stirring is done at a rate of approximately 60 revolutions per minute.
4.     The test flame is applied at intervals depending upon the expected flash and fire points and corresponding temperatures at which the material shows the sign of flash and fire are noted.

Observations: -
TABLE 4.4: - Observations of Flash Point of bitumen sample taken
Test
Trial 1
Trial 2
Trial 3
Mean value
Flash Point ( 0C )
253
251
250
251.33

Result: The temperature at which the flame application that causes a bright flash  251.330C.

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